The TGA excess weight improve curve is proven in Determine 1. The 1st fat loss action may be the volatilization accompanied by A significant decomposition action. The spinoff of bodyweight modify curve in eco-friendly reveals a peak exactly where the height max is at 427.seventy one ˚C. The MS data is gathered all over the entire TGA experiment. Ion currents and TGA mass reduction are plotted being a perform of temperature (see Determine two). It is crucial to keep in mind that the products and solutions of a TGA test are Usually decomposition solutions, and that's correct in these experiments likewise. As a result, the purpose is to comprehend the thermal degradation goods of nylon sixty six. TGA-MS consistently monitors the decomposition off gases being a functionality of time and temperature. The degradation mechanism with the polymer molecules breaking at the C-N bond produces more compact polymer molecules Along with the exact device of bicarbonyl polymethylene fragments as well as fragments will break down into carbon dioxide, carbon monoxide, drinking water, and hydrocarbons [five].

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The degradation of nylon sixty six Within this Section of the research was also carried out on a TGA5500. The off-fuel solutions were being analyzed employing a FTIR for that IR spectra plus a GC/MS for your MS Examination.

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The TGA-FTIR benefits compliment the TGA-MS outcomes. Both procedures give beneficial information about the buildings on the off-gas goods through the nylon 66 thermal degradation system. FTIR can be quite useful to detect the existence of particular chemical bonds plus some practical groups in polymers. It can be extensively useful for polymer characterization.